++1 on using white vinegar, I’ve done it many times, and doing it now as we speak to a 550 tank.
I let the vinegar sit in the sun for a few days (or even a week of really bad), then throw a few handfuls of big bolts (smaller ones may get lodged in the corners of the tank). I’ve also used copper BB’s to agitate, but those don’t scrape as much as nuts and bolts.